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Best Practices
Interlaboratory Proficiency Testing Program Best Practices
In the course of the ongoing proficiency test program, it is probable that new information will arise that will shed light on the effectiveness of current testing practices. Properly used, this will lead to the development of improved testing practices. With a significantly large population of laboratories participating, all of whom are accredited to the highest standard, there is a unique opportunity to draw meaningful conclusions about the best methodology or nuances of technique to apply in the future.
This information might suggest ways to improve accuracy or reliability of data produced or generate new consensus positions on current requirements. Proposals for entirely new technologies might be discussed, tested and critically reviewed by the Nadcap laboratory community.
After a proposal has been thoroughly reviewed and verified by the Task Group, a suggested practices document or other appropriate reference materials will be published in this location. This will provide an added value to all participants in the Nadcap process, which is not achievable in any other forum.
This forum provides a uniquely focused place for consensus to be sought and improvements generated that serves the needs of aerospace labs, without the compromises intrinsic to technical bodies with a more general orientation.
If you would like to participate in the generation or peer review of publications, or to suggest a best practice, please contact:
Jim Lewis, Senior Staff Engineer + 1 724 772 1616 extension 8688
Jennifer Kornrumpf, CSR + 1 724 772 1616 extension 8680
Accepted Best Practices for Interlaboratory Prociency Testing Program
CHEMISTRY
Nickel Base Alloys, Cobalt Base Alloys, High Alloy Iron Base Alloys • Major Elements and Minor Elemental Constituents – XRF • Trace Elements – Graphite Furnace Atomic Absorption, ICP
Low Alloy Iron Base, Titanium Base Alloys • Major Elements and Minor Elemental Constituents – XRF, OES • Trace Elements – Graphite Furnace Atomic Absorption, ICP
Aluminium Base Alloys • Major Elements and Minor Elemental Constituents – XRF • Trace Elements – Graphite Furnace Atomic Absorption
Magnesium Base Alloys, Copper Base Alloys • Major Elements and Minor Elemental Constituents – XRF • Trace Elements – Graphite Furnace Atomic Absorption
MECHANICAL
| Room Temperature Tensile |
ASTM E8 |
| Elevated Temperature Tensile |
ASTM E21 |
| Stress Rupture |
ASTM E139 (Smooth) / ASTM E292 (Notched) |
| Creep |
ASTM E139 |
| Impact Testing |
ASTM E23 |
| High Cycle Fatigue (HCF) |
ASTM E466 |
| Low Cycle Fatigue (LCF) |
ASTM E606 |
| Fracture Toughness |
ASTM E399 |
| Crack Propagation |
ASTM E647 |
| Cyclic Rupture |
ASTM E139 |
| Bend Test |
ASTM E290 |
METALLOGRAPHY AND MICROHARDNESS (Metallic Materials)
Metallography (General Interior)
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ASTM E3 - Preparation of Metallographic Specimens ASTM E112 - Grain Size Measurement |
| Titanium Microstructures |
AMS 2380 |
| Metallography (Macro) |
ASTM E340 – Macroetching of Metallographic Speciments |
Microexamination: Surface Conditions • Alloy Depletion • Oxidation / Corrosion Layers • Casting Surface Reactions (Mold Reactions) • Diffusion Coatings (Carburizing, Nitriding) • Intergranular Attack / Intergranular Oxidation (IGA/IGO) • Alpha Case on Titanium Alloys (Cast/Wrought/Thermal Processes)
Microhardness • Anoop • Vickers
(Applied loads of less than 1 kgf performed on mounted and metallographically polished specimens)
- Interior
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ASTM E384 |
| - Surface |
ASTM E384 |
HARDNESS
Brinell
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ASTM E10 |
| Rockwell |
ASTM E18 |
| Vickers (Macro) |
ASTM E92 (applied loads of 1 kgf to 120 kgf) |
DIFFERENTIAL THERMAL ANALYSIS
• Differential Thermal Analysis MECHANICAL TEST SPECIMEN PREPARATION
Low Stress Grinding & Polishing
Residual Stress: X-Ray Diffraction
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